80 FR 32114 - Office of Research and Development; Ambient Air Monitoring Reference and Equivalent Methods: Designation of One New Reference Method and Four New Equivalent Methods

ENVIRONMENTAL PROTECTION AGENCY

Federal Register Volume 80, Issue 108 (June 5, 2015)

Page Range		32114-32116
FR Document		2015-13800

Notice is hereby given that the Environmental Protection Agency (EPA) has designated, in accordance with 40 CFR part 53, one new reference method and one new equivalent for measuring concentrations of PM<INF>2.5</INF>, one new equivalent method for measuring PM<INF>10-2.5,</INF> and two new equivalent methods for measuring ozone (O<INF>3</INF>) in the ambient air.

Federal Register, Volume 80 Issue 108 (Friday, June 5, 2015)

[Federal Register Volume 80, Number 108 (Friday, June 5, 2015)]
[Notices]
[Pages 32114-32116]
From the Federal Register Online  [www.thefederalregister.org]
[FR Doc No: 2015-13800]


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ENVIRONMENTAL PROTECTION AGENCY

[FRL-9928-61-ORD]


Office of Research and Development; Ambient Air Monitoring 
Reference and Equivalent Methods: Designation of One New Reference 
Method and Four New Equivalent Methods

AGENCY: Environmental Protection Agency (EPA).

ACTION: Notice of designation of one reference method and three 
equivalent methods for monitoring ambient air quality.

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SUMMARY: Notice is hereby given that the Environmental Protection 
Agency (EPA) has designated, in accordance with 40 CFR part 53, one new 
reference method and one new equivalent for measuring concentrations of 
PM2.5, one new equivalent method for measuring 
PM10-2.5, and two new equivalent methods for measuring ozone 
(O3) in the ambient air.

FOR FURTHER INFORMATION CONTACT: Robert Vanderpool, Human Exposure and 
Atmospheric Sciences Division (MD-D205-03), National Exposure Research 
Laboratory, U.S. EPA, Research Triangle Park, North Carolina 27711. 
Email: Vanderpool.Robert@epa.gov.

SUPPLEMENTARY INFORMATION: In accordance with regulations at 40 CFR 
part 53, the EPA evaluates various methods for monitoring the 
concentrations of those ambient air pollutants for which EPA has 
established National Ambient Air Quality Standards (NAAQSs), as set 
forth in 40 CFR part 50. Monitoring methods that are determined to meet 
specific requirements for adequacy are designated by the EPA as either 
reference methods or equivalent methods (as applicable), thereby 
permitting their use under 40 CFR part 58 by States and other agencies 
for determining compliance with the NAAQSs.
    The EPA hereby announces the designation of one new reference 
method for measuring PM2.5, one new equivalent method for 
measuring PM2.5, one new equivalent method for measuring 
PM10-2.5, and two equivalent methods for measuring ozone 
(O3) in the ambient air. These designations are made under 
the provisions of 40 CFR part 53, as amended on August 31, 2011 (76 FR 
54326-54341).
    The new reference method for PM2.5 is a manual 
monitoring method based on a particular PM2.5 sampler and is 
identified as follows:

[[Page 32115]]

    RFPS-0315-221, ``Met One Instruments, Inc. e-FRM,'' configured for 
filter sampling of ambient particles using the US EPA PM10 
inlet specified in 40 CFR 50 Appendix L, Figs. L-2 thru L-19, equipped 
with either a BGI VSCC\TM\ cyclone or WINS PM2.5 
fractionator, with a flow rate of 16.67 L/min, using 47 mm PTFE 
membrane filter media, and operating with firmware version R1.1.0 and 
later, and operated in accordance with the Met One e-FRM 
PM2.5 operating manual.
    The application for reference method determination for the 
PM2.5 method was received by the Office of Research and 
Development on January 9, 2015. This monitor is commercially available 
from the applicant, Met One Instruments, Inc., 1600 Washington Blvd., 
Grants Pass, OR 97526.
    The new PM2.5 Class II equivalent method is nearly 
identical to a corresponding Tisch Environmental Inc. sampler (RFPS-
1014-219) that had been previously designated by EPA as a reference 
method sampler for PM2.5. The significant difference is that 
the newly designated PM2.5 equivalent method sampler is 
configured to use a Tisch Environmental Inc. Model TE-PM2.5C cyclone as 
the principle size separator (fractionator) for the sampler rather than 
the WINS impactor or the BGI VSCC^TM used in the 
corresponding PM2.5 reference method sampler. The newly 
designated Class II equivalent method is identified as follows:
    EQPS-0415-223 ``Tisch Environmental Model TE-Wilbur2.5 
PM2.5 Low-Volume Air Particulate Sampler,'' configured as a 
PM2.5 equivalent method, with firmware version 1.70 or later 
and a TE-PM10-D PM10 size-selective inlet as specified in 40 
CFR 50 Appendix L Figs. L-2 thru L-19, configured with a Tisch TE-
PM2.5C particle size separator, and operated for 24-hour continuous 
sample periods at a flow rate of 16.67 L/min, using 47 mm PTFE membrane 
filter media, operated with or without the optional TE-W-600 Solar 
Panel Power Supply kit, and in accordance with the Tisch Environmental 
Model TE-Wilbur2.5 PM2.5 Low-Volume Air Particulate Sampler 
instruction manual and with the requirements and sample collection 
filters as specified in 40 CFR part 50, Appendix L.
    In the particular case of the new Tisch Class II PM2.5 
equivalent method, a corresponding Tisch Environmental Inc. 
PM2.5 reference method sampler (RFPS-1014-219) may be 
converted to the equivalent method configuration by replacement of the 
WINS impactor or the VSCC^TM cyclone with the Tisch 
Environmental TE-PM2.5C cyclone specified in the equivalent method 
description. The TE-PM2.5C device should be purchased from the sampler 
manufacturer, who will also furnish installation, conversion, 
operation, and maintenance instructions for the TE-PM2.5C, as well as a 
new equivalent method identification label to be placed on the sampler. 
If the conversion is to be permanent, the original designation 
reference method label should be removed from the sampler and replaced 
with the new designated equivalent method label. In the case where a 
converted sampler may need to be restored later to its original 
reference method configuration (such as for an application specifically 
requiring a reference method) by re-installation of the WINS impactor 
or the VSCC^TM cyclone, the new equivalent method label may 
be installed on the sampler without removing the original reference 
method label, such that the sampler bears both labels. In this 
situation, the sampler shall be clearly and conspicuously marked by the 
operator to indicate its current configuration (i.e. WINS reference 
method, VSCC^TM reference method, or TE-PM2.5C equivalent 
method) so that the monitoring method is correctly identified and the 
correct method code is used when reporting monitoring data obtained 
with the sampler.
    The new PM10-2.5 equivalent method utilizes a pair of 
filter samplers, one of which has been designated as an equivalent 
method for PM2.5, and one which has been designated as a 
reference method for PM10. Both samplers have been shown to 
meet the requirements specified in Appendix O of 40 CFR part 50. The 
PM2.5 equivalent method sampler and the PM10 
reference method sampler are designated as EQPS-0415-223 and RFPS-0714-
216, respectively. The newly designated PM10-2.5 equivalent 
method sampler is identified as follows:
    EQPS-0415-224, ``Tisch Environmental Model TE-Wilbur Low-Volume Air 
Particulate Sampler Pair'' for the determination of coarse particulate 
matter as PM10-2.5, consisting of a pair of Tisch 
Environmental Model TE-Wilbur samplers, with one being the TE-Wilbur2.5 
PM2.5 sampler with TE-PM2.5C particle size separator (EQPS-
0415-223) and the other being a TE-Wilbur10 PM10 sampler 
(RFPS-0714-216), and operated in accordance with the associated TE-
Wilbur instruction manual. This designation applies to 
PM10-2.5 measurements only.
    The application for equivalent method Class II determination for 
the PM2.5 method was received by the Office of Research and 
Development on July 21, 2014 and the PM10-2.5 method 
application was received on April 21, 2015. These samplers are 
commercially available from the applicant, Tisch Environmental, Inc., 
145 S. Miami Avenue, Village of Cleves, OH 45002.
    The two new equivalent methods for ozone are both automated 
monitoring methods (analyzers) utilizing ultraviolet absorption 
photometry and are identified as follows:
    EQOA-0415-222, ``Sutron Model 6030 Ozone Analyzer,'' operated at 
any of the following measurement ranges: 0-0.05 ppm, 0-0.5 ppm and 0-
1.0 ppm, at any ambient temperature in the range of 5 [deg]C-45 [deg]C, 
with an averaging time of 1 to 99 analyzer cycles (0 to 396 seconds), 
with sample flow rate of 0.5 to 1 Lpm and in accordance with the Model 
6030 Ozone Analyzer Operation Manual and with or without the following 
options: Internal ozone generator, zero/span ports for external 
calibration.
    This application for equivalent method determination for the ozone 
method was received by the Office of Research and Development on March 
9, 2015. This monitor is commercially available from the applicant, 
Sutron Air Quality Division, 2548 Shell Road, Georgetown, TX 78628.
    EQOA-0515-225 ``Environnement S.A. Model O3 42e UV Photometric 
Ozone Analyzer,'' operated in a range of 0-0.5 ppm in an environment of 
0-35 [deg]C, with a Teflon sample inlet filter, with automatic 
temperature and pressure compensation, with zero/span external solenoid 
valve, with automatic or fixed response time, and with or without the 
following options: ESTEL Analog Input/Output Board, LCD color touch 
screen, and internal ozone generator.
    The application for equivalent method determination for the ozone 
method was received by the Office of Research and Development on April 
20, 2015. This analyzer is commercially available from the applicant, 
Environnement S.A., 111, Boulevard Robespierre, 78300 Poissy France.
    Test monitors representative of these methods have been tested in 
accordance with the applicable test procedures specified in 40 CFR part 
53, as amended on August 31, 2011. After reviewing the results of those 
tests and other information submitted in the application, EPA has 
determined, in accordance with Part 53, that these methods should be 
designated as equivalent methods.
    As designated reference and equivalent methods, these methods are 
acceptable for use by states and other air monitoring agencies under 
the requirements of 40 CFR part 58,

[[Page 32116]]

Ambient Air Quality Surveillance. For such purposes, the methods must 
be used in strict accordance with the operation or instruction manual 
associated with the method and subject to any specifications and 
limitations (e.g., configuration or operational settings) specified in 
the applicable designated method description (see the identification of 
the method above).
    Use of the methods also should be in general accordance with the 
guidance and recommendations of applicable sections of the ``Quality 
Assurance Handbook for Air Pollution Measurement Systems, Volume I,'' 
EPA/600/R-94/038a and ``Quality Assurance Handbook for Air Pollution 
Measurement Systems, Volume II, Ambient Air Quality Monitoring 
Program'' EPA-454/B-08-003, December, 2008. Provisions concerning 
modification of such methods by users are specified under Section 2.8 
(Modifications of Methods by Users) of Appendix C to 40 CFR part 58.
    Consistent or repeated noncompliance should be reported to: 
Director, Human Exposure and Atmospheric Sciences Division (MD-E205-
01), National Exposure Research Laboratory, U.S. Environmental 
Protection Agency, Research Triangle Park, North Carolina 27711.
    Designation of these reference and equivalent methods is intended 
to assist the States in establishing and operating their air quality 
surveillance systems under 40 CFR part 58. Questions concerning the 
commercial availability or technical aspects of the method should be 
directed to the applicant.

    Dated: May 20, 2015.
Jennifer Orme-Zavaleta,
Director, National Exposure Research Laboratory.
[FR Doc. 2015-13800 Filed 6-4-15; 8:45 am]
BILLING CODE 6560-50-P

Federal Register / Vol. 80, No. 108 / Friday, June 5, 2015 / Notices 32115

RFPS–0315–221, ‘‘Met One specified in the equivalent method 21, 2014 and the PM10-2.5 method
Instruments, Inc. e-FRM,’’ configured description. The TE–PM2.5C device application was received on April 21,
for filter sampling of ambient particles should be purchased from the sampler 2015. These samplers are commercially
using the US EPA PM10 inlet specified manufacturer, who will also furnish available from the applicant, Tisch
in 40 CFR 50 Appendix L, Figs. L–2 thru installation, conversion, operation, and Environmental, Inc., 145 S. Miami
L–19, equipped with either a BGI maintenance instructions for the TE– Avenue, Village of Cleves, OH 45002.
VSCCTM cyclone or WINS PM2.5 PM2.5C, as well as a new equivalent The two new equivalent methods for
fractionator, with a flow rate of 16.67 method identification label to be placed ozone are both automated monitoring
L/min, using 47 mm PTFE membrane on the sampler. If the conversion is to methods (analyzers) utilizing ultraviolet
filter media, and operating with be permanent, the original designation absorption photometry and are
firmware version R1.1.0 and later, and reference method label should be identified as follows:
operated in accordance with the Met removed from the sampler and replaced EQOA–0415–222, ‘‘Sutron Model
One e-FRM PM2.5 operating manual. with the new designated equivalent 6030 Ozone Analyzer,’’ operated at any
The application for reference method method label. In the case where a of the following measurement ranges: 0–
determination for the PM2.5 method was converted sampler may need to be 0.05 ppm, 0–0.5 ppm and 0–1.0 ppm, at
received by the Office of Research and restored later to its original reference any ambient temperature in the range of
Development on January 9, 2015. This method configuration (such as for an 5 °C–45 °C, with an averaging time of 1
monitor is commercially available from application specifically requiring a to 99 analyzer cycles (0 to 396 seconds),
the applicant, Met One Instruments, reference method) by re-installation of with sample flow rate of 0.5 to 1 Lpm
Inc., 1600 Washington Blvd., Grants the WINS impactor or the VSCCTM and in accordance with the Model 6030
Pass, OR 97526. cyclone, the new equivalent method Ozone Analyzer Operation Manual and
The new PM2.5 Class II equivalent label may be installed on the sampler with or without the following options:
method is nearly identical to a without removing the original reference Internal ozone generator, zero/span
corresponding Tisch Environmental Inc. method label, such that the sampler ports for external calibration.
sampler (RFPS–1014–219) that had been bears both labels. In this situation, the This application for equivalent
previously designated by EPA as a sampler shall be clearly and method determination for the ozone
reference method sampler for PM2.5. The conspicuously marked by the operator method was received by the Office of
significant difference is that the newly to indicate its current configuration (i.e. Research and Development on March 9,
designated PM2.5 equivalent method WINS reference method, VSCCTM 2015. This monitor is commercially
sampler is configured to use a Tisch reference method, or TE–PM2.5C available from the applicant, Sutron Air
Environmental Inc. Model TE–PM2.5C equivalent method) so that the Quality Division, 2548 Shell Road,
cyclone as the principle size separator monitoring method is correctly Georgetown, TX 78628.
(fractionator) for the sampler rather than identified and the correct method code EQOA–0515–225 ‘‘Environnement
the WINS impactor or the BGI VSCCTM is used when reporting monitoring data S.A. Model O3 42e UV Photometric
used in the corresponding PM2.5 obtained with the sampler. Ozone Analyzer,’’ operated in a range of
reference method sampler. The newly The new PM10-2.5 equivalent method 0–0.5 ppm in an environment of 0–35
designated Class II equivalent method is utilizes a pair of filter samplers, one of °C, with a Teflon sample inlet filter,
identified as follows: which has been designated as an with automatic temperature and
EQPS–0415–223 ‘‘Tisch equivalent method for PM2.5, and one pressure compensation, with zero/span
Environmental Model TE-Wilbur2.5 which has been designated as a external solenoid valve, with automatic
PM2.5 Low-Volume Air Particulate reference method for PM10. Both or fixed response time, and with or
Sampler,’’ configured as a PM2.5 samplers have been shown to meet the without the following options: ESTEL
equivalent method, with firmware requirements specified in Appendix O Analog Input/Output Board, LCD color
version 1.70 or later and a TE–PM10–D of 40 CFR part 50. The PM2.5 equivalent touch screen, and internal ozone
PM10 size-selective inlet as specified in method sampler and the PM10 reference generator.
40 CFR 50 Appendix L Figs. L–2 thru method sampler are designated as The application for equivalent
L–19, configured with a Tisch TE– EQPS–0415–223 and RFPS–0714–216, method determination for the ozone
PM2.5C particle size separator, and respectively. The newly designated method was received by the Office of
operated for 24-hour continuous sample PM10-2.5 equivalent method sampler is Research and Development on April 20,
periods at a flow rate of 16.67 L/min, identified as follows: 2015. This analyzer is commercially
using 47 mm PTFE membrane filter EQPS–0415–224, ‘‘Tisch available from the applicant,
media, operated with or without the Environmental Model TE–Wilbur Low- Environnement S.A., 111, Boulevard
optional TE–W–600 Solar Panel Power Volume Air Particulate Sampler Pair’’ Robespierre, 78300 Poissy France.
Supply kit, and in accordance with the for the determination of coarse Test monitors representative of these
Tisch Environmental Model TE– particulate matter as PM10-2.5, consisting methods have been tested in accordance
Wilbur2.5 PM2.5 Low-Volume Air of a pair of Tisch Environmental Model with the applicable test procedures
Particulate Sampler instruction manual TE–Wilbur samplers, with one being the specified in 40 CFR part 53, as amended
and with the requirements and sample TE–Wilbur2.5 PM2.5 sampler with TE– on August 31, 2011. After reviewing the
collection filters as specified in 40 CFR PM2.5C particle size separator (EQPS– results of those tests and other
part 50, Appendix L. 0415–223) and the other being a TE– information submitted in the
In the particular case of the new Tisch Wilbur10 PM10 sampler (RFPS–0714– application, EPA has determined, in
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Class II PM2.5 equivalent method, a 216), and operated in accordance with accordance with Part 53, that these
corresponding Tisch Environmental Inc. the associated TE–Wilbur instruction methods should be designated as
PM2.5 reference method sampler (RFPS– manual. This designation applies to equivalent methods.
1014–219) may be converted to the PM10-2.5 measurements only. As designated reference and
equivalent method configuration by The application for equivalent equivalent methods, these methods are
replacement of the WINS impactor or method Class II determination for the acceptable for use by states and other air
the VSCCTM cyclone with the Tisch PM2.5 method was received by the Office monitoring agencies under the
Environmental TE–PM2.5C cyclone of Research and Development on July requirements of 40 CFR part 58,

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32116 Federal Register / Vol. 80, No. 108 / Friday, June 5, 2015 / Notices

Ambient Air Quality Surveillance. For title, EPA ICR Number and OMB practical utility; (ii) evaluate the
such purposes, the methods must be Control Number provided in the text) to accuracy of the Agency’s estimate of the
used in strict accordance with the the Office of Management and Budget burden of the proposed collection of
operation or instruction manual (OMB) for review and approval in information, including the validity of
associated with the method and subject accordance with the Paperwork the methodology and assumptions used;
to any specifications and limitations Reduction Act (44 U.S.C. 3501 et seq.). (iii) enhance the quality, utility, and
(e.g., configuration or operational Before doing so, EPA is soliciting public clarity of the information to be
settings) specified in the applicable comments on specific aspects of the collected; and (iv) minimize the burden
designated method description (see the proposed information collection as of the collection of information on those
identification of the method above). described below. These are proposed who are to respond, including through
Use of the methods also should be in extensions of the currently approved the use of appropriate automated
general accordance with the guidance ICRs. An Agency may not conduct or electronic, mechanical, or other
and recommendations of applicable sponsor and a person is not required to technological collection techniques or
sections of the ‘‘Quality Assurance respond to a collection of information other forms of information technology,
Handbook for Air Pollution unless it displays a currently valid OMB e.g., permitting electronic submission of
Measurement Systems, Volume I,’’ EPA/ control number. responses. Burden is defined at 5 CFR
600/R–94/038a and ‘‘Quality Assurance DATES: Comments must be submitted on 1320.03(b). EPA will consider the
Handbook for Air Pollution or before August 4, 2015. comments received and amend the ICR
Measurement Systems, Volume II, ADDRESSES: Submit your comments, as appropriate. The final ICR package
Ambient Air Quality Monitoring referencing the Docket ID numbers will then be submitted to OMB for
Program’’ EPA–454/B–08–003, provided for each item in the text, review and approval. At that time, EPA
December, 2008. Provisions concerning online using www.regulations.gov (our will issue another Federal Register
modification of such methods by users preferred method), by email to notice to announce the submission of
are specified under Section 2.8 docket.oeca@epa.gov, or by mail to: EPA the ICR to OMB and the opportunity to
(Modifications of Methods by Users) of Docket Center, Environmental submit additional comments to OMB.
Appendix C to 40 CFR part 58. Protection Agency, Mail Code 28221T, General Abstract: For all the listed
Consistent or repeated noncompliance 1200 Pennsylvania Ave. NW., ICRs in this notice, owners and
should be reported to: Director, Human Washington, DC 20460. operators of affected facilities are
Exposure and Atmospheric Sciences EPA’s policy is that all comments required to comply with reporting and
Division (MD–E205–01), National received will be included in the public record keeping requirements for the
Exposure Research Laboratory, U.S. docket without change including any general provisions of 40 CFR part 60,
Environmental Protection Agency, personal information provided, unless subpart A or Part 63, Subpart A, as well
Research Triangle Park, North Carolina the comment includes profanity, threats, as the applicable specific standards.
27711. information claimed to be Confidential This includes submitting initial
Designation of these reference and Business Information (CBI) or other notifications, performance tests and
equivalent methods is intended to assist information whose disclosure is periodic reports and results, and
the States in establishing and operating restricted by statute. maintaining records of the occurrence
their air quality surveillance systems FOR FURTHER INFORMATION CONTACT: and duration of any startup, shutdown,
under 40 CFR part 58. Questions Patrick Yellin, Monitoring, Assistance, or malfunction in the operation of an
concerning the commercial availability and Media Programs Division, Office of affected facility, or any period during
or technical aspects of the method Compliance, Mail Code 2227A, which the monitoring system is
should be directed to the applicant. Environmental Protection Agency, 1200 inoperative. These reports are used by
Dated: May 20, 2015. Pennsylvania Ave. NW., Washington, EPA to determine compliance with the
Jennifer Orme-Zavaleta, DC 20460; telephone number: (202) standards.
Director, National Exposure Research 564–2970; fax number: (202) 564–0050; (1) Docket ID Number: EPA–HQ–
Laboratory. email address: yellin.patrick@epa.gov. OECA–2011–0271; Title: NESHAP for
[FR Doc. 2015–13800 Filed 6–4–15; 8:45 am] SUPPLEMENTARY INFORMATION: Integrated Iron and Steel Manufacturing
Supporting documents which explain in (40 CFR part 63, subpart FFFFF); EPA
BILLING CODE 6560–50–P
detail the information that the EPA will ICR Number 2003.06, OMB Control
be collecting are available in the public Number 2060–0517; Expiration Date:
ENVIRONMENTAL PROTECTION docket for this ICR. The docket can be October 31, 2015.
AGENCY viewed online at www.regulations.gov Respondents: Integrated iron and steel
or in person at the EPA Docket Center, plants.
[FRL–9928–74–OECA] Respondent’s obligation to respond:
EPA West, Room 3334, 1301
Constitution Ave. NW., Washington, Mandatory (40 CFR part 63, subpart
Proposed Information Collection FFFFF).
Request; Comment Request; See Item DC. The telephone number for the
Docket Center is 202–566–1744. For Estimated number of respondents: 18
Specific ICR Titles Provided in the (total).
Text; See the Item Specific Docket additional information about EPA’s
public docket, visit http://www.epa.gov/ Frequency of response: Initially,
Numbers Provided in the Text
dockets. occasionally and semiannually.
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AGENCY: Environmental Protection Pursuant to section 3506(c)(2)(A) of Estimated annual burden: 18,421
Agency (EPA). the PRA, EPA is soliciting comments hours.
ACTION: Notice. and information to enable it to: (i) Estimated annual cost: $1,832,122,
Evaluate whether the proposed includes $67,002 annualized capital or
SUMMARY: The Environmental Protection collection of information is necessary operation & maintenance (O&M) costs.
Agency (EPA) is planning to submit the for the proper performance of the Changes in Estimates: There is no
below listed information collection functions of the Agency, including change in burden hours from the
requests (ICR) (See item specific ICR whether the information will have previous ICR.

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Document Created: 2015-12-15 15:20:47
Document Modified: 2015-12-15 15:20:47

Category		Regulatory Information
Collection		Federal Register
sudoc Class		AE 2.7: GS 4.107: AE 2.106:
Publisher		Office of the Federal Register, National Archives and Records Administration
Section		Notices
Action		Notice of designation of one reference method and three equivalent methods for monitoring ambient air quality.
Contact		Robert Vanderpool, Human Exposure and Atmospheric Sciences Division (MD-D205-03), National Exposure Research Laboratory, U.S. EPA, Research Triangle Park, North Carolina 27711. Email: [email protected]
FR Citation		80 FR 32114